Date of Award

August 2023

Degree Type

Dissertation

Degree Name

Doctor of Philosophy

Department

Engineering

First Advisor

Deyang Qu

Committee Members

Xiaoli Ma, Benjamin Church, Yonjin Sung, Illya Avdeev

Abstract

Dendrite growth is a major obstacle to the commercialization of Li metal batteries. A dendrite formed on a Li anode can cause thermal run-aways and permanent capacity loss. An in-situ optical techniques is considered as one of the major methods to study the dendrites growth behaviors and morphologies real-time. A home-designed in-situ optical cell with a digital optical microscope was used to investigate the behavior of Li deposition on a metallic Li electrode under different electrochemical operation conditions. The impacts of electrolytes, additives and cycling conditions on the dendrite formation were investigated. Guiding by the in-situ optical observation results, polycyclic aromatic hydrocarbons (PAHs) were introduced as additives to suppress the dendrite growth by forming a dynamic elastic protection layer and reacting with newly deposited dendrites. The in-situ observation method of solid-state electrolyte is also introduced.

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